Trimethylsilylation of a variety of alcohols and phenols, in the presence of silica chloride, using hexamethyldisilazane (HMDS) in solution and under solvent-free conditions is reported. Trimethylsilyl ethers were formed in excellent yields both for aliphatic alcohols and phenols without having an electron-withdrawing group. In addition, SiO2-Cl can be recovered and reused after drying.
. (2006). Silylation of Alcohols and Phenols Using HMDS Catalyzed by SiO2-Cl in Solution and Solvent-Free Conditions. (e31729). Journal of Sciences, Islamic Republic of Iran, 17(2), e31729
MLA
. "Silylation of Alcohols and Phenols Using HMDS Catalyzed by SiO2-Cl in Solution and Solvent-Free Conditions" .e31729 , Journal of Sciences, Islamic Republic of Iran, 17, 2, 2006, e31729.
HARVARD
. (2006). 'Silylation of Alcohols and Phenols Using HMDS Catalyzed by SiO2-Cl in Solution and Solvent-Free Conditions', Journal of Sciences, Islamic Republic of Iran, 17(2), e31729.
CHICAGO
, "Silylation of Alcohols and Phenols Using HMDS Catalyzed by SiO2-Cl in Solution and Solvent-Free Conditions," Journal of Sciences, Islamic Republic of Iran, 17 2 (2006): e31729,
VANCOUVER
. Silylation of Alcohols and Phenols Using HMDS Catalyzed by SiO2-Cl in Solution and Solvent-Free Conditions. J. Sci. I. R. I.. 2006;17(2):e31729.
Journal of Sciences, Islamic Republic of Iran